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UKAEA-CCFE-PR(24)2402023
In this study, we compare the formation of radiation induced defects in W and W-Re-Os alloys, exposed to an equivalent dose of self-ion and neutron irradiation. Transmutation reactions in the neutron irradiated material are simulated in the ion implanted materials by alloying with representative quantities of Re and Os (1.4 and 0.1 at.% respecti…
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UKAEA-CCFE-PR(24)2392021
One of the main capabilities of Atom Probe Tomography (APT) is the ability to not only identify but characterise early stages of precipitation at scales that are not achievable by other techniques. The most popular method, based on the Density-Based Spatial Clustering of Applications with Noise (DBSCAN), is used extensively in many branches of r…
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UKAEA-CCFE-PR(21)492021
Using a combination of simulated data and pyrite isotopic reference materials, we have refined a methodology to obtain quantitative δ34S measurements from atom probe tomography (APT) datasets. This study builds on previous attempts to characterize relative 34S/32S ratios in gold containing pyrite using APT. We have also improved our understand…
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UKAEA-CCFE-PR(19)422019
High temperature, neutron irradiated single crystal tungsten, with a post irradiation composition of W-1.20±0.11at.%Re-0.11±0.05at.%Os-0.03±0.01at.%Ta was characterised using a combination of Atom Probe Tomography (APT) and Scanning Transmission Electron Microscopy (STEM). APT showed that within nanoscale clusters of Re/Os, the atomic density wa…
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